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Leak Detection in Pressurised Devices: The Sensitive Test

By Dr Graham Rogers
EMEA-Leybold-Phoenix

Devices operating above atmospheric pressure, such as valves for the oil and gas industry, are an important application of leak detection. Other uses include checking the leak integrity of containers holding biological and nuclear substances, and even the performance of car tyres. Here's a quick overview of the sensitive test of a helium checker fundamental to leak detection in pressurised devices.

 

There are many ways of leak detecting, such as bubble test or pressure drop, but none can compete with the sensitivity and the ability to pinpoint a leak that a Helium leak checker can offer. Additionally such an instrument allows both quantitative and qualitative measurements.

A helium or, more precisely, a Helium 4 leak detector is essentially a tuned mass spectrometer which detects this gas and has the further option of identifying Helium 3 (used in cryogenics) and hydrogen. The unit has appropriate pumps supplied making it portable, with only mains electricity required. The unit is extremely sensitive to helium.

Investigating leaks in these circumstances can involve both a qualitative and a quantitative approach and just as in vacuum applications a helium leak detector is essential. Depending on the specification leaks rates below 10-6 mbar l/s are frequently required. Helium leak checkers with an ultimate sensitivity of 10-12 mbar l/s offer the most accurate solution.

Related: Don't let your research be at risk of a leaky vacuum chamber. Watch the webinar in which our in-house leak detection expert, Mike Ridenour, shares what he's learn in his 40 years' experience in vacuum and leak detection, and how you can avoid common errors when leak testing. 

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Why we use Helium as the search gas

There are several key benefits of using Helium as the search gas:

  • It is non-toxic
  • Relatively low cost
  • Only 5 ppm occurs naturally in air
  • It is one of the smallest atoms, resulting in the ability to investigate small leaks
  • It is a low-density gas which easily disperses

Related: Vacuum Science World shared a great article on Helium leak detection methods. Find the blog post here, Four Ways of Finding Vacuum Leaks Using Helium

 

Two ways of using the Helium leak detector

The schematic below shows the leak checker operating in a quantitative or integral mode to determine the total leak rate of a component. This value will determine the overall lifetime, say, of containers for hazardous gases and liquids. In the case of car tyres, in general their pressure is not checked on a regular basis. Thus the correct leak rate will ensure the pressure loss is sufficiently low over a period of several months to guarantee that there are no safety issues.

EMEA-OverpressureMethod-IntegralDetection
You will note that depending on the size of the test chamber additional pumps might be required to pump the chamber to below 10-3 mbar to ensure the unit is operating at its most sensitive range. However this means not all the helium is detected by the leak checker. To determine the correct leak rate, the pumping ratios of the leak detector and chamber pumps must be factored in to give an accurate reading.

If the component is of sufficient value to warrant re-working, the actual leaks can be determined by operating the detector in what is known as “sniffer mode”, using a sniffer attached to the inlet port of the leak detector and pressuring the component with helium. The illustration below gives a typical set up:

EMEA-OverpressureMethod-LocalDetection

In this mode a probe with a small orifice is connected to the inlet of the leak detector by flexible vacuum hose, typically 4 m in length. The size of the orifice governs the flow of detected helium so that the inlet pressure to the instruments is kept below 10-3 mbar, allowing accurate measurements of leak rates. This has the following advantages:

  • Exact location of leaks is determined
  • It performs in a qualitative mode
  • No additional pumps are required
  • Actual flow out of the object is measured, simulating real leakage from the device

A sniffer with an additional pump allows a hose length of 20 m in length

You will note that the minimum detection level in this case is 1x10-7 mbar l/s. This is a consequence of air having a natural concentration of 5 ppm of helium, which gives a less sensitive detection level than the local mode described previously. However for many applications this can be acceptable.

More on Leak Detection

There's more to leak detection than just a Helium leak checker. Dive into more detail on our resource page (which you can also download as a free ebook) by clicking the link below. 

Explore the Resource Page

 

The fundamentals of leak detection

Tags: Leak Detection

About Dr Graham Rogers

Dr Graham Rogers
Dr Graham Rogers has extensive experience across the world of vacuum, having been involved in the detailed specification and technical selling of the complete range of products, principally for Leybold, over the past 30 years. He brings in-depth knowledge from the metallurgy, chemical, analytical, R&D and semiconductor sectors, and has a passion for helping customers in solving problems and developing solutions that will bring real process improvements and value. Graham is a science graduate from Oxford University, UK, where he gained his degree in Chemistry and a DPhil in Physical Chemistry. His journey into vacuum science began early on in his career when worked developing semiconductor processes particularly thin film coating, this led him into the exciting and inspiring world of vacuum and eventually Leybold. We are delighted to have Graham as a resident Consultant for Leybold, where he is able to share his knowledge and insight through our vacuum academy training, videos and blogs.

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